2种储存温度对牙本质黏结剂黏结强度的影响

上海口腔医学 ›› 2013, Vol. 22 ›› Issue (6): 659-661.

2种储存温度对牙本质黏结剂黏结强度的影响

张晓，王庆，薛苗苗，刘一凡

(郑州大学第四附属医院修复科，河南郑州 450052)

收稿日期:2013-03-18 修回日期:2013-04-26 出版日期:2013-04-12 发布日期:2013-04-12
通讯作者: 张晓,Tel:0371-66993400,E-mail:zhangxiaoxiao67@126.com
作者简介:张晓(1967-)，女，硕士，副教授

Effect of bonding strength of dentin adhesive agent under 2 kinds of storage temperatures

ZHANG Xiao, WANG Qing, XUE Miao-miao, LIU Yi-fan

Department of Prosthodontics, the Fourth Affiliated Hospital, Zhengzhou University. Zhengzhou 450052, Henan Province, China

Received:2013-03-18 Revised:2013-04-26 Online:2013-04-12 Published:2013-04-12

摘要/Abstract

摘要： 目的：研究不同储存温度对牙本质黏结剂黏结强度的影响。方法：将100颗离体牙随机分为10组，每组10颗，再随机将每组10颗牙分A、B 2组，每组5颗。第1周黏结时，黏结剂未做温度差别处理，从第2周开始，每组的 A组为4℃冷藏黏结剂处理组，B组为25℃室温存储黏结剂处理组。在10周内分别对离体牙进行树脂黏结处理，制成试件，用万能材料测试仪以1 mm/min速度测试剪切力，采用SPSS 18.0软件包对数据进行单因素方差分析和LSD t检验。结果：分别对A、B 2个实验组的剪切力值进行单因素方差分析，差异有显著性(P<0.05)。进一步采用LSD t检验进行组间比较，结果显示，前5周差异均无显著性，第6～10周，差异均有显著性。结论：随着时间的延长，冷藏组与室温组的牙本质黏结剂的黏结强度呈下降趋势，从第6周开始，冷藏组与室温组的牙本质黏结剂的黏结强度的差异逐渐明显。

关键词: 牙本质黏结剂 , 储存温度, 黏结强度

Abstract: PURPOSE: To measure the changes of bonding strength of dentin adhesive agent at different storage temperatures. METHODS: One hundred extracted bicuspids were randomly divided into 10 sets, 10 teeth in each set. Each set was further divided randomly into Group A and Group B, each with 5 teeth. During a 10-week test period, Groups A and B were applied with adhesives labeled A and B. Group A was refrigerated under 4℃ and B was stored at room-temperature from the second week on. The first set was stored at the same situation. The shear force of samples were tested by universal material tester at the speed of 1 mm/min. The results were evaluated using one-way ANOVA and LSD t test using SPSS 18.0 software package. RESULTS: According to one-way ANOVA, the shear bond strength of the 2 groups differed significantly(P<0.05). Comparing the sets by LSD t test, the results showed that during the first 5 weeks, there was no significant difference between Group A and B. However, there were measurable differences in performance after 6 weeks. CONCLUSIONS: With time goes on, the bonding strength of both refrigerated and room-temperature adhesives tend to diminish. After 6 weeks, the bonding performance of the 2 groups begins to differ significantly, and the refrigerated adhesives are superior to room-temperature adhesives.

Key words: Dentin adhesive agent, Storage temperature, Bonding strength

中图分类号:

R783.1

张晓, 王庆, 薛苗苗, 刘一凡. 2种储存温度对牙本质黏结剂黏结强度的影响[J]. 上海口腔医学, 2013, 22(6): 659-661.

ZHANG Xiao, WANG Qing, XUE Miao-miao, LIU Yi-fan. Effect of bonding strength of dentin adhesive agent under 2 kinds of storage temperatures[J]. Shanghai Journal of Stomatology, 2013, 22(6): 659-661.

参考文献

[1] Ye Q, Park JG, Topp E, et al. In vitro performance of nano-heterogeneous dentin adhesive[J]. J Dent Res,2008,87(9):829-833.
[2] 王粉琼, 肖玉鸿, 贾安琦. 牙本质黏结体系中单体水解和析出的机制及其影响因素[J]. 牙体牙髓牙周病学杂志, 2013, 23(1): 57-60.
[3] Ye Q, Park J, Laurence JS, et al. Ternary phase diagram of model dentin adhesive exposed to over-wet environments[J]. J Dent Res, 2011, 90(12): 1434-1438.
[4] Haller B, Hofmann N, Klaiber B, et al. Effect of storage media on microleakage of five dentin bonding agents[J]. Dent Mater, 1993, 9(3): 191-197.
[5] Pashley DH, Sano H, Ciucchi B, et al. Adhesion testing of dentin bonding agents: a review[J]. Dent Mater, 1995, 11(2): 117-125.
[6] Cehreli ZC, Kecik D, Kocadereli I. Effect of self-etching primer and adhesive formulations on the shear bond strength of orthodontic brackets[J]. Am J Orthod Dentofacial Orthop, 2005, 127(5): 573-579.
[7] Buonocore MG. A simple method of increasing the adhesion of acrylic filling materials to enamel surfaces[J]. J Dent Res, 1955, 34(6): 849-853.
[8] Yahagi C, Takagaki T, Sadr A, et al. Effect of lining with a flowable composite on internal adaptation of direct composite restorations using all-in-one adhesive systems[J]. Dent Mater J, 2012, 31(3): 481-488.
[9] 黄翠, 程祥荣. 牙本质黏结剂的回顾现状和展望[J]. 中华口腔医学杂志, 2006, 41(11): 700-701.
[10] Nishiyama N, Tay FR, Fujita K, et al. Hydrolysis of functional monomers in a single-bottle self-etching primer--correlation of 13C NMR and TEM findings[J]. J Dent Res,2006,85(5):422-426.
[11] Yamauti M, Hashimoto M, Sano H, et al. Degradation of resin-dentin bonds using NaOCl storage[J]. Dent Mater, 2003, 19(5): 399-405.
[12] Ma S, Nakajima KF, Nishiyama N. Effects of storage temperature on the shelf life of one-step and two-step self-etch adhesives[J]. Oper Dent, 2009, 34(4): 472-480.
[13] Fujita K, Nishiyama N. 13C NMR analysis of the etching efficacyof acidic monomers in self-etching primers[J]. J Dent,2006,34(2): 123-133.
[14] Kazantsev OA, Shirshin KV, Sivokhin AP, et al. Hydrolysis of 2-hydroxyethyl methacrylate in concentrated aqueous solutions[J]. Russian J Appl Chem, 2003, 76(8): 1296-1298.