Shanghai Journal of Stomatology ›› 2015, Vol. 24 ›› Issue (6): 679-686.

• Basic study • Previous Articles     Next Articles

Sintering behavior of tooth-like yttria-stabilized tetragonal zirconia polycrystal by adding rare-earth oxide

GAO Yan1, ZHANG Fu-qiang1, GAO Jian-hua2.   

  1. 1.Department of Prosthodontics, Shanghai Ninth People’s Hospital, College of Stomatology, Shanghai Jiao Tong University School of Medicine;
    Shanghai Key Laboratory of Stomatology. Shanghai 200011;
    2.Shanghai Institute of Ceramics, Chinese Academy of Sciences. Shanghai 200050, China
  • Received:2015-02-10 Online:2015-12-25 Published:2016-01-04
  • Contact: 上海市科学技术委员会生物医药重点项目(09411954600);上海高校选拔培养优秀青年教师科研专项基金(jdy09046) E-mail:drgaoyan@gmail.com

Abstract: PURPOSE To investigate the influence on the sintering densification, microstructure and transformation behavior of tooth-like yttria-stabilized tetragonal zirconia polycrystal by adding rare-earth oxide as colorants. METHODS Six kinds(S1,S2,S3,S4,S5,S6) of tooth-like yttria stabilized tetragonal zirconia polycrystal(Y-TZP)were made by introducing internal colorating technology, the relative density of sintered specimens was determined by the Archimedes method. Scanning electron microscope (SEM) was used to examine the surface morphology and determine the grain size. The phase identification of sintered samples was carried out by X-ray diffractometer. RESULTS The relative density of the six kinds of tooth-like yttria stabilized tetragonal zirconia polycrystal were over 98%,through SEM images of the cross-sectional surfaces, the grain size of the six kinds of sintered composites were observed in a wide range from 100 nm to 300 nm, a second phase was not detected in the grain boundaries. The diffraction peaks of the main phase were observed as tetragonal phase.CONCLUSIONS Tooth-like yttria-stabilized tetragonal zirconia polycrystal was acquired with better mechanical property by adding rare-earth oxide as colorants, and was available for clinical application.

Key words: Tetragonal zirconia polycrystal, Rare earth oxide, Sintering behavior, Microstructure, X-ray diffractometer

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